Characterization of Zinc Oxide (ZnO) Thin Films Prepared by RF-Sputtering, Sol-Gel, and Evaporation Methods for Optoelectronic Applications
DOI:
https://doi.org/10.32628/IJSRST2613373Keywords:
ZnO tetraleg, RF-sputtering, Evaporation method, XRD, PL spectroscopyAbstract
The structural and optical properties of Zinc Oxide (ZnO) thin films fabricated on silicon (Si) substrates using prepared by Radio-Frequency (RF) Sputtering, Sol-Gel (spin coating) and Evaporation methods have been studied and investigated. X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Atomic Force Microscopy (AFM), and Photoluminescence (PL) spectroscopy were used for comprehensive characterization. ZnO thin film prepared using thermal evaporation method has referred a narrow FWHM, large grain size, rough surface morphology and low tensile strain compared with the ZnO thin film prepared using RF-sputtering and sol-gel method, which may be of advantage in absorbing UV light when used as a UV detector. Additionally, the ZnO tetraleg structures are uniform and are 2.5 nm in length and 0.12 µm in width. Finally, two luminescence peaks in UV and visible region can be observed of ZnO/Si (110) thin film prepared using RF-sputtering, sol-gel and thermal evaporation methods with different peaks of intensity. blue shift with respect to energy band gap of sample prepared by thermal evaporation has been obtained.
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K.M. Lee, CW. Lai, K.S. Ngai & J.C. Juan,’’ Recent developments of zinc oxide based photocatalyst in water treatment technology’’: A review, Water Res., Vol. 88, pp. 428–448, 2016.
L. Qia., A. Zhu, W. Zeng, R. Dong, P. Tan, Z. Ding , P. Gao, S. Wang & J. Pan, ’’Achieving electronic structure reconfiguration in metallic carbides for robust electrochemical water splitting’’, Journal of Materials Chemistry A.,no.5,pp. 2453–2462, Feb 2020
F. Pan, C. Song, X.J. Liu, Y.C. Yang, F. Zeng,’’ Ferromagnetism and possible application in spintronics of transition-metal-doped ZnO films’’, Mater. Sci. Eng. R vol. 62, pp. 1–35, Apr 2008.
D. Sridevi, K.V. Rajendran,’’Synthesis and optical characteristics of ZnO nanocrystals’’, Journal of Bull. Mater. Sci., Vol. 32, No. 2, pp. 165–168, Apr 2009.
J. H. Lee, K. h. Ko, B.O. Park ,’’ Electrical and optical properties of ZnO transparent conduction films by the sol-gel method’’, Journal of Crystal Growth ,Vol. 247, No. 1-2, pp.119-125, Jan 2003.
E. sub, S.H.S. kang, J.S. Kang ,J.H. kim, S.Y. Lee,’’ Effect of the variation of film thickness on the structural and optical properties of ZnO thin film deposited on sapphire substrate using PLD’’, Applied Surface Science, Vol.186, No. 1, pp. 474-476, Jan 2002.
C. C. Lin, S. K. Tsai, M. Y. Chang, ’’ Spontaneous Growth by Sol-Gel Process of Low Temperature ZnO as Cathode Buffer Layer in Flexible Inverted Organic Solar Cells’’. Journal of Organic Electronics, Vol. 46, pp. 218–225, July 2017.
P. Rong, S. Ren, &, Q. Yu,’’ Fabrications and Applications of ZnO Nanomaterials in Flexible Functional Devices-A Review’’, Journal of Critical Reviews in Analytical Chemistry, Vol. 49, No. 4, pp. 336–349, Dec 2018.
X. Jiang, F.L. Wong, M.K. Fung, S.T. Lee,’’ Aluminum-doped zinc oxide films as transparent conductive electrode for organic light-emitting devices’’ , Journal of Appl. Phys. Lett. , Vol.83, No. 9, pp. 1875- 1877, Sep 2003.
G. Aygun, I. Yildiz, ’’ Interfacial and structural properties of sputtered HfO2 Layers’’, Journal of Appl. Phys., Vol.106, No. 1, July 2009.
H. Belaid, M. Nouiri, A. Sayari, et al.’’ Structural and electrical characterizations of ZnO:In/PS/Si heterojunction deposited by rf-magnetron sputtering’’. Journal of Electroceram, Vol. 35, No. 1, pp. 141–147, Dec 2015.
S.A. Maky, B.K. Hassun, T.H. Mahmoud, ’’ Study of the effect of thickness on the structural properties and optical constants of cadmium selenide (CdSe) thin films’’ , Journal of the College of Education, vol.18, no.1, pp. 249–26, 2017.
B.D. Yao, Y.F. Chan, N Wang,’’ Formation of ZnO nanostructures by a simple way of thermal evaporation’’, Journal of Applied Physics Letters, Vol.81, No. 4, pp. 757-759, July 2002.
H. Lv, D. Sang, H. Li, et al.’’ Thermal Evaporation Synthesis and Properties of ZnO Nano/Microstructures Using Carbon Group Elements as the Reducing Agents’’. Journal of Nanoscale Res Lett , Vol.5,No.3, pp. 620, Jan 2010.
I. A. Abbas, S. Q. Hazaa, “Study the Effect of Etching Time on the Characteristics of the Porous Silicon that Prepare from N-Type Silicon by Photoelectrochemical Etching Method ", Al-Mustansiriya Journal of Science and Education, Vol. 23, No.2, Apr 2022.
A. Sh. Hussein, Z. Hassan, S. M. Thahab, S. S. Ng, H. A. Hassan & C. W. Chin,’’Effect of Al Mole Fraction on Structural and Electrical Properties of AlxGa1-xN/GaN Heterostructures Grown by Plasma-assisted Molecular Beam Epitaxy’’, Journal of Appl. Surf. Sci., Vol.257, No.9, pp. 4159-4164, Feb 2011.
W. A. Fadhil, T. J. Alwan, ’’ Effect of TiO2 on the Optical Properties of ANI/TiO2 Nanocomposite Thin Films’’, Al-Mustansiriya Journal of Science and Education, Vol. 22, No.4, Dec 2021.
R. Ghosh, D. Basak, S. Fujihara,’’ Effect of substrate-induced strain on the structural, electrical, and optical properties of polycrystalline ZnO thin films’’, Journal of Applied Physics , Vol. 96, No. 5, pp. 2689–2696, 2004.
X. W. Sun, H. S. kwork,’’ Optical properties of epitaxially grown zinc oxide films on sapphire by pulsed laser deposition’’, Journal of Applied Physic, Vol. 86,No. 1, pp. 408-411, 1999.
I. H. Khudayer, A.A. Shehab, ’’ Study of the effect of annealing temperature on the structural and optical properties of ZnSe octahedral’’, Ibn Al-Haitham J. for Pure & Appl. Sci., Vol. 28, No. 1, 2015.
H. I. Abdulgafour, S. M. Abdalhadi, M. H. Mahmood, ’’Synthesis and characterization of ZnO tetrapod-like nanorods without catalyst by wet thermal evaporation and applied on dye-sensitized solar cells’’, Int. J. Mod. Phys. B, Vol. 39, No. 8, 2025.
M. H. M. Yusoff, S. M. S. M. Rahim, A. R. M. Radzol, K. A. A. Wahid, M. H. A. Wahid, "Fabrication and Performance of UV Photodetector Based on Nanostructure ZnO Thin-Film Deposited by Vacuum Coating Technique," IEEE Xplore, 2016
S. N. A. Sultanov, Z. X. Mirzajonov, F. T. Yusupov, T. I. Rakhmonov, "Nanocrystalline ZnO Films on Various Substrates: A Study on Their Structural, Optical, and Electrical Characteristics", East European Journal of Physics, No. 2, pp. 309-314, 2024
Kanthakhoo, N. (2024). Exosomal Immune Checkpoint Molecules as Liquid Biopsy Markers. Available at SSRN 6466858.
M. M. Abdullah, F. M. Al-Marzouki, A. A. Al-Ghamdi, "Optical and structural characterization of ZnO thin films prepared by thermal evaporation method," Materials Research Express, Vol. 12, No. 2, 2025
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